Water‐Stable,Magnetic Silica–Cobalt/Cobalt Oxide–Silica Multishell Submicrometer Spheres

A method to produce monodisperse magnetic composite spheres with diameters from less than 100 nm to more than 1 μm in water solution is reported. The spheres consist of a dielectric silica core and a cobalt/cobalt oxide shell which can be protected from further oxidation with an outer shell of silica or, alternatively, they can be covered with the polymer polyvinylpyrrolidone as a stabilizer. The formation of a uniform magnetic shell proceeds with the adsorption of metallic cobalt seeds, produced by the reduction of cobalt chloride with sodium borohydride, on a self‐assembled layer of polyelectrolytes on the silica core. In the second step, an outer silica shell can be formed by the hydrolysis and condensation of (3‐aminopropyl)trimethoxysilane and tetraethoxysilane. The double‐shell composite spheres show excellent sphericity, monodispersity, and a magnetic hysteresis loop at room temperature.     

EXPERIMENTAL STUDIES AND NUMERICAL CALCULATION ON TURBULENT BOUNDARY LAYER OF WATER FLOW ALONG CURVED SURFACE

This paper will introduce experimental studies and numerical calculation onturbulent boundary layer of water flow along curved surface in our country in recent years.Onthe basis of the experimental studies,the effects of curvature and roughness on velocitydistribution and pressure distribution and the change of turbulent flow boundary layer onoverflow bucket concave surface is discussed.We proposed the empirical formula of velocity,pressure and the change of turbulent flow boundary layer on outlet bucket concave.According tothe momentum principle,we have deduced the momentum integral equation full water depthboundary layer and using the element as control unit inside the boundary layer on concavesurface of bucket.Combining with continuity equation,we have computed the boundary layerdevelopment on the bucket of a spillway.Compared with the field experimental data,thecalculation results are available.Under polar coordinates,a mathematical model for simulatingtime-averaged flow characteristics in concave surface of bucket is established.The turbulent flowfield on concave surface of bucket is calculated by SIMPLE method and this mathematicalmodel.The flow velocity field,pressure field,distribution of turbulent kinetic energy,distribution of turbulent energy dissipating rate and distribution of shear stress are available.Thecalculation value is consistent with measured test data.     

Determination of the width of the transition layer between the crystalline and amorphous zones in nylon 1010 by SAXS

The width of the transition layer between the crystalline and amorphous zones in nylon 1010 was determined by SAXS with point collimation and long-slit collimation, respectively. The width of the transition layer, E, was found to be 1.7 nm. The results show that the width of the transition layer is independent of crystallinity.     

单层球面网壳地震反应特征分析

考虑不同矢跨比、荷载、跨度和支座刚度等多种因素的影响,对单层球面网壳在地震作用下的反应进行了较全面的研究,给出了其随各参数变化的规律,得出了在单层球面网壳抗震设计中起控制作用的是水平地震作用而不是竖向地震作用等有益的结论.此外本文还给出了由于阻尼比不同而需对引用现行抗震规范反应谱分析的网壳地震作用进行修正的建议.     

聚氨酯泡沫夹克管生产材料的代用

介绍一种用于生产聚氨酯泡沫夹克管保温层的新材料聚酯聚醚，报道选用这种材料生产泡沫夹克管的工艺及工要工艺参数和产品达到的技术指标及现场应用情况。     

平面分层介质结构全波分析综述

本文综述了广义谱域导抗法，直线法及直线法的快速算法，全波离散镜象法等主要方法，并对各种方法的特点进行了比较，这些方法可有效地处理平面分层介质结构问题，文中包括作者近期的研究成果。     

薄层反射波非零炮检距的属性特征

 本文从薄层顶、底界面反射波的走时入手，研究了薄层反射波在非零炮检距集上出现的干涉现象，导出了薄层反射波在出现干涉时的炮检距计算公式，说明薄层干涉出现的炮检距是多变量函数，即随着埋藏深度h、地层速度v、薄层厚度Δh以及地震波的主频f*的变化而改变。本文重点分析了地层厚度Δh和地震子波主频f*对反射波振幅特性和频率特性的影响。在充分分析薄层反射的振幅、频谱随炮检距变化关系的基础上，指出在应用叠前信息（如AVO分析）进行储层预测等方面的研究时，应充分考虑薄层反射波的干涉和调谐现象带来的振幅和频率特征的变化。     

不同灌溉条件下的水稻需水规律及水分生产率分析

稻田需水量包括植株蒸腾、棵间蒸发、田间渗漏3部分。研究表明，水稻在充分供水条件下所形成的蒸腾量中包含了一部分无效蒸腾，无效蒸腾量的减少不会影响作物的生长发育，反而会有不同程度的增产和优质效应。节水灌溉技术的推广产生了明显的经济与社会效益。结合当地实际情况采用3种常见的灌溉方式探讨了不同灌溉方式下水稻的需水规律、灌概定额和生产率的差异，为水稻节水高效栽培提供理论与技术依据。     

反向凝固法生产H90-钢-H90复合带

研究H90-钢-H90反向凝固复合过程中复合层厚度的变化规律以及复合带的组织和性能，探讨界面结合机理。结果表明：随着浸渍时间的增加，复合层的厚度变化经历了凝固生长、平衡相持和回熔3个阶段，钢带的预热温度越低，获得的最大复合层厚度越厚；H90复合层的组织为等轴晶粒，复合界面处Cu和Fe发生了扩散，而Zn未发生明显扩散，扩散层较薄，约为4μm；复合带的界面结合牢固；不同复合层厚度的复合带，其力学性能略有差异，但均达到GB5213——85所规定的F级深冲钢板的力学性能要求。